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Heating causes the crystal structure of the mineral (or minerals) to degrade, and, as the sample melts, trapped gases are released.
Different minerals have different closure temperatures; biotite is ~300°C, muscovite is about 400°C and hornblende has a closure temperature of ~550°C.
Similarly, the Permian-Triassic extinction is now dated at 252.5 Ma, which is effectively coincident with the age determined by other means for Siberian Traps basalt flows.
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